HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68619724, compound → HCID 11291335, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68619724 | HCID 68619724 | — |
| Solvent | Ethanol heptane | HCID 22502148 | — |
| Product | HCID 11291335 | HCID 11291335 | — |
Reaction Steps
(RS,RS,RS)-[9,10-Dimethoxy-3-(2-oxo-piperidin-1-yl)-1,3,4,6,7,11b-hexahydro-2H-pyrido[2,1-a]isoquinolin-2-yl]-carbamic acid tert-butyl ester (580 mg, 1.61 mmol) was dissolved in ethanol/heptane 3:2 (5 mL) and subjected to preparative HPLC (Chiralpak® AD column, heptane/ethanol 80:20).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07122555B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-b6aee979175f4432b18d59fdd310c2e9 |
| Source note | uspto-grants-2006_10 |