HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11291335, compound → HCID 11337326, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11291335 | HCID 11291335 | — |
| Solvent | Ethanol heptane | HCID 22502148 | — |
| Product | HCID 11337326 | HCID 11337326 | — |
Reaction Steps
Light yellow semisolid, 220 mg (38%), tR=32.0 min (Chiralpak® AD 25×0.46 cm, heptane/ethanol 80:20, flow rate 1 mL/min). (+)-(R,R,R)-1-(2-Amino-9,10-dimethoxy-1,3,4,6,7,11b-hexahydro-2H-pyrido [2,1-a]isoquinolin-3-yl)-piperidin-2-one: Light yellow semisolid, 207 mg (36%), tR=55.4 min (Chiralpak® AD 25×0.46 cm, heptane/ethanol 80:20, flow rate 1 mL/min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07122555B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-1528c565d17941e681853c7e34cf333d |
| Source note | uspto-grants-2006_10 |