HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-bromo-N-(4-methylpent-2-yn-4-yl)butyramide → 2-(3,8-dibromo-6-quinolinyloxy)-N-(4-methylpent-2-yn-4-yl) butyramide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-bromo-N-(4-methylpent-2-yn-4-yl)butyramide | HCID 21078406 | — |
| Reactant | 3,8-Dibromo-6-hydroxyquinoline | HCID 21923136 | — |
| Product | 2-(3,8-dibromo-6-quinolinyloxy)-N-(4-methylpent-2-yn-4-yl) butyramide | HCID 69253886 | — |
Reaction Steps
In a similar procedure, 3,8-dibromo-6-hydroxyquinoline was reacted with 2-bromo-N-(4-methylpent-2-yn-4-yl) butyramide to give 2-(3,8-dibromo-6-quinolinyloxy)-N-(4-methylpent-2-yn-4-yl) butyramide as a colourless gum, 1H NMR (CDCl3) δ: 1.07(3H, t); 1.59 (3H, s); 1.60(3H, s); 1.78(3H, s); 1.99–2.06(2H, m); 4.52(1H, t); 6.30(1H, s); 7.00(1H, m); 7.82(1H, dd); 8.21(1H, d); 8.88(1H, m).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07122672B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-7b32c218b2df4edca33614b9f20c263d |
| Source note | uspto-grants-2006_10 |