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HRID1244863

反应详情

EQUATION

反应方程式

HRID 1244863 的结构方程式

REACTANTS

反应物

2
结构：C=C(C)C(=O)O
HCID4093

Methacrylic acid

C4H6O2

结构：CC(=O)O[Si](C)(C)C
HCID75988

Silanol, 1,1,1-trimethyl-, 1-acetate

C5H12O2Si

PRODUCTS

生成物

1
结构：C=C(C)C(=O)O[Si](C)(C)C
HCID2733839

2-Propenoic acid, 2-methyl-, trimethylsilyl ester

C7H14O2Si

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCCCCC
溶剂HCID8058

n-Hexane

C6H14

PROCEDURE

实验过程

20 ml of acetoxytrimethylsilane and 11.4 ml of commercial methacrylic acid (ATOFINA Norsocryl® MAA) in 100 ml of hexane are mixed and heated. Azeotropic distillation of acetic acid affords trimethylsilyl methacrylate.

WORKUP

后处理

  1. temperatureheated
  2. distillationAzeotropic distillation of acetic acid