HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methacrylic Acid → 2-Propenoic acid, 2-methyl-, trimethylsilyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methacrylic Acid | HCID 4093 | — |
| Reactant | Silanol, 1,1,1-trimethyl-, 1-acetate | HCID 75988 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | 2-Propenoic acid, 2-methyl-, trimethylsilyl ester | HCID 2733839 | — |
Reaction Steps
20 ml of acetoxytrimethylsilane and 11.4 ml of commercial methacrylic acid (ATOFINA Norsocryl® MAA) in 100 ml of hexane are mixed and heated. Azeotropic distillation of acetic acid affords trimethylsilyl methacrylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07122692B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-84921c3b361f4ad9a245e308e86de751 |
| Source note | uspto-grants-2006_10 |