HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acrylic Acid → Tri-isopropyl silyl acrylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acrylic Acid | HCID 6581 | — |
| Reactant | HCID 21923867 | HCID 21923867 | — |
| Solvent | Toluene | HCID 1140 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | Tri-isopropyl silyl acrylate | HCID 167468 | — |
Reaction Steps
4 g of acetoxy-triisopropylsilane and 1.6 g of acrylic acid (ATOFINA Norsocryl AA®) in 100 ml of toluene and 1 mL of N,N-dimethylformamide are mixed and heated. Azeotropic distillation of acetic acid affords triisopropylsilyl acrylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07122692B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-1ee8f1dcc122490b89368cae55c6565d |
| Source note | uspto-grants-2006_10 |