反应详情

温度

97.5 °C

120 mg of the product obtained in Stage 1 above, 2 ml of butanol and 0,105 ml of benzylamine are mixed together and the reaction medium is heated to a temperature of approximately 95 to 100° C. for 10 hours. It is then left to return to ambient temperature and diluted with 5 ml of isopropanol, followed by separating, washing with 5 ml of isopropanol and drying under vacuum at approximately 30° C. In this way 132 mg of expected product is obtained in the form of white crystals.

1. waitIt is then left
2. customto return to ambient temperature
3. customby separating
4. washwashing with 5 ml of isopropanol
5. customdrying under vacuum at approximately 30° C