HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 21923032, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | HCID 21923063 | HCID 21923063 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 21923032 | HCID 21923032 | 87.4% |
Reaction Steps
The operation is carried out as in Stage 2 of Example 2 from 200 mg (0.77 mM) of the product obtained in Stage 1 of Example 2 and 3 ml of butanol and using 0.088 ml of aniline (0.96 mmole) in place of the benzylamine. In this way 213 mg of expected product is obtained in the form of white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07122669B1 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-6caae1a9fd254690bc611d780eb3f475 |
| Source note | uspto-grants-2006_10 |