HuagongsheHuagongshe Chemistry Print Report · For research reference only
(S)-1-Benzyl 2-methyl 4-methylenepyrrolidine-1,2-dicarboxylate → HCID 57457963, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (S)-1-Benzyl 2-methyl 4-methylenepyrrolidine-1,2-dicarboxylate | HCID 54190049 | — |
| Reactant | HCID 69558490 | HCID 69558490 | — |
| Product | HCID 57457963 | HCID 57457963 | 24% |
Reaction Steps
In a similar manner to the procedures described in Preparative Examples 8(ii)′, 8(iii)′, 8(iv)′, 8(v)′ and 8(vi)′ above, reactions were conducted in turn, using (S)-1-benzyloxycarbonyl-4-propylideneproline methyl ester [prepared as described in Preparative Example 25′ above] instead of (S)-1-benzyloxycarbonyl-4methylideneproline methyl ester, to give the title compound as a brown oil (yield: 24%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07122666B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-1b6aececcaa848c4904cf1cdbfaf06f3 |
| Source note | uspto-grants-2006_10 |