HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21919190, compound → HCID 21919141, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21919190 | HCID 21919190 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21919141 | HCID 21919141 | 97% |
Reaction Steps
Methyl 4-(3,4,5,6-tetramethoxy-2-methylbenzyl)-2-benzyloxybenzoate (530 mg, 1.1373 mmol) was dissolved in methanol (20 ml), added to a methanolic suspension (20 ml) of 10% palladium-carbon (100 mg) and stirred for 16 hours at room temperature in a hydrogen atmosphere. The reaction solution was filtered and the filtrate was concentrated under reduced pressure to give the title compound (414 mg, 1.101 mmol, 97%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07122543B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-9697c94361b74267b360774a048f9c55 |
| Source note | uspto-grants-2006_10 |