HCID 178447847, compound → HCID 178447848, compound

Participants

Reaction Steps

A mixture of 2,5-difluoro(4-(trans-4-propylcyclohexyl)cyclohexenyl)benzene (0.84 mmol), ethyl acetate (30 ml), and 5% palladium carbon (0.013 g) is stirred under an atmosphere of hydrogen. After ceasing the absorption of hydrogen, 5% palladium carbon is filtered off from the reaction mixture. The filtrate is concentrated under reduced pressure and purified by silica-gel chromatography, and further recrystallized to give the titled compound.

Provenance & Evidence