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HRID1245322

反应详情

EQUATION

反应方程式

HRID 1245322 的结构方程式

REACTANTS

反应物

3
结构：Cc1ccccc1
HCID1140

Toluene

C7H8

结构：CC1(c2ccccc2)NC(=O)NC1=O
HCID93043

5-Methyl-5-phenylhydantoin

C10H10N2O2

结构：CCCc1c(OCCCCBr)ccc2c(C(F)(F)F)noc12
HCID21910990

未命名化合物

PRODUCTS

生成物

1
结构：CCCc1c(OC(C)CCN2C(=O)NC(C)(c3ccccc3)C2=O)ccc2c(C(F)(F)F)noc12
HCID21911005

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)=O
溶剂HCID180

Acetone

C3H6O

PROCEDURE

实验过程

rac-5-Methyl-5-phenyl-3-(3-{[7-propyl-3-(trifluoromethyl)-1,2-benzisoxazol-6-yl]oxy}butyl)imidazolidine-2,4-dione was prepared as for Example 10 from 5-methyl-5-phenylimidazolidine-2,4-dione and the bromide from Example 8. After aqueous work-up and silica gel chromatography (toluene: 10% acetone), the title compound was obtained.