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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1245443Generated: October 25, 2026

Di-tert-butyl Iminodicarboxylate → Di(tert-butyl) 3-cyanobenzylimidodicarbonate

https://huagongshe.com/reaction/1245443

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDi-tert-butyl IminodicarboxylateHCID 279800—
Reactant3-(Chloromethyl)benzonitrileHCID 522126—
ProductDi(tert-butyl) 3-cyanobenzylimidodicarbonateHCID 21930987—

Reaction Steps

) 3-(Chloromethyl)benzonitrile (30 g; 197.9 mmol) and di-tert-butyl iminodicarboxylate were reacted in analogy to Lila et al., Synth. Comm. 28, 23, 1998, 4419, to give di(tert-butyl) 3-cyanobenzylimidodicarbonate. 65 g of a reddish oil were obtained and were employed without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07125883B1
Source datasetuspto-grants-2006_10
ORD IDord-c4d609bb29c8458cb2217ade58ca1743
Source noteuspto-grants-2006_10