HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylurea → HCID 21912490, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylurea | HCID 10853 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethylacetate methanol | HCID 21584119 | — |
| Product | HCID 21912490 | HCID 21912490 | — |
Reaction Steps
) 4 g of benzylurea 14a were dissolved in a mixture of ethyl acetate/CH3OH 3:1 with heating and, after addition of 0.2 g of 10% Pd on activated carbon, hydrogenated under standard conditions at 35 to 40° C. After the reaction was complete, the mixture was filtered through Celite and evaporated. 2.8 g; ESI-MS [M+H+]=248.15
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07125883B1 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-0e4cf875518540669772ea0743a6916d |
| Source note | uspto-grants-2006_10 |