Methylhydrazine → HCID 21912777, compound

HRID 1245590Notes

Reaction equation

HRID 1245590 reaction equation
[NH:1]1[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[CH3:7][NH:8][NH2:9].F[C:11](F)(F)[CH2:12]NN>>[CH3:7][N:8]1[C:12]([CH:4]2[CH2:5][CH2:6][NH:1][CH2:2][CH2:3]2)=[C:11]2[C:2]([CH2:3][CH2:4][CH2:5][CH2:6]2)=[N:9]1

Participants

4

Reactant 3

HCID 6061MethylhydrazineHCID 8082PiperidineHCID 787402,2,2-Trifluoroethylhydrazine

Product 1

HCID 21912777HCID 21912777, compound

Procedure

The title compound was prepared using procedures analogous to that described for Piperidine 11, except methylhydrazine was substutited for (2,2,2-trifluoroethyl)hydrazine. 1H-NMR (500 MHz) δ 1.69–1.89 (m, 8H), 2.33 (br m, 1H), 2.57–2.78 (m, 7H), 3.18–3.21 (m, 2H), 3.77 (s, 3H).

Sources & evidence

ORD record
ord-af788ef0485a417ab7c19a7e4855bdea
Source dataset
uspto-grants-2006_10
Patent number
US07125887B2

Reaction notes

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