HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → 4-(1-Ethyl-3-methoxy-4-methyl-1H-pyrazol-5-yl)piperidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | HCID 21912745 | HCID 21912745 | — |
| Product | 4-(1-Ethyl-3-methoxy-4-methyl-1H-pyrazol-5-yl)piperidine | HCID 21912771 | — |
Reaction Steps
The title compound was prepared from 1-tert-butoxycarbonyl-4-(1-ethyl-3-methoxy-4-methyl-(1H)-pyrazol-5-yl)piperidine (Step E) using a procedure analogous to that described for Piperidine 14, Step F. 1H-NMR (500 MHz) δ 1.33 (t, J=7.1, 3H), 1.70–1.73 (m, 2H), 1.86–1.96 (m, 5H), 2.67–2.72 (m, 3H), 3.19–3.21 (m, 2H), 3.89 (s, 3H), 3.99 (q, J=7.1, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07125887B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-ef3ce89c10c841fb9fe394575e071bdd |
| Source note | uspto-grants-2006_10 |