HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-2-methylbenzenesulfonyl chloride → 3-Chloro-N-(4-ethyl-1,3-thiazol-2-yl)-2-methylbenzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-2-methylbenzenesulfonyl chloride | HCID 522734 | — |
| Reactant | 4-Ethyl-1,3-thiazol-2-amine | HCID 12378205 | — |
| Product | 3-Chloro-N-(4-ethyl-1,3-thiazol-2-yl)-2-methylbenzenesulfonamide | HCID 9879979 | 17% |
Reaction Steps
The title compound was prepared from 4-ethyl-1,3-thiazol-2-ylamine (METHOD H) and 3-chloro-2-methylbenzenesulfonyl chloride according to METHOD A, yellowish solid, 53 mg (17% yield): HRMS Calcd (found) for C12H13ClN2O2S2 m/z 316.0107 (316.0120).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07125900B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-78aa7a900dd542d88c4f608993ebed80 |
| Source note | uspto-grants-2006_10 |