HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-2-methylbenzenesulfonyl chloride → HCID 9902066, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-2-methylbenzenesulfonyl chloride | HCID 522734 | — |
| Reactant | 4-Propyl-2-thiazolamine | HCID 12779875 | — |
| Product | HCID 9902066 | HCID 9902066 | 39% |
Reaction Steps
The title compound was prepared from 4-propyl-1,3-thiazol-2-ylamine (METHOD I) and 3-chloro-2-methylbenzenesulfonyl chloride according to METHOD A, yellow solid, 90 mg (39% yield): mp 169° C.; HRMS Calcd (found) for C13H15ClN2O2S2 M/Z 330.0263 (330.0251).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07125900B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-bbabb1fcce904aaca8998f147f08b9da |
| Source note | uspto-grants-2006_10 |