HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-2-methylbenzenesulfonyl chloride → HCID 10269059, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-2-methylbenzenesulfonyl chloride | HCID 522734 | — |
| Reactant | 4-tert-Butyl-1,3-thiazol-2-amine | HCID 2734202 | — |
| Product | HCID 10269059 | HCID 10269059 | 40% |
Reaction Steps
The title compound was prepared from 4-tert-butyl-1,3-thiazol-2-ylamine (METHOD H) and 3-chloro-2-methylbenzenesulfonyl chloride according to METHOD A, white foam, 273 mg (40% yield). mp 178° C.; HRMS Calcd (found) for C14H17ClN2O2S2 m/z 344.0420 (344.0408).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07125900B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-5496c0b9d1ff45ac9a91e2d3af8efcfd |
| Source note | uspto-grants-2006_10 |