HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzenesulfonyl chloride → N-(5-acetyl-4-methyl-1,3-thiazol-2-yl)-4-chlorobenzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzenesulfonyl chloride | HCID 7398 | — |
| Reactant | 5-Acetyl-2-amino-4-methylthiazole | HCID 720882 | — |
| Product | N-(5-acetyl-4-methyl-1,3-thiazol-2-yl)-4-chlorobenzenesulfonamide | HCID 11163340 | — |
Reaction Steps
The title compound was prepared from 5-acetyl-2-amino-4-methylthiazole and 4-chlorobenzenesulfonyl chloride as described in the synthetic METHOD B to give a white solid (12.2 mg) with purity >90%. LCMS (pos) m/z 331.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07125900B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-704ed33f3c1d41f5adb539d08d6d101e |
| Source note | uspto-grants-2006_10 |