HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-2,5-difluorobenzenesulfonyl Chloride → HCID 11200726, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-2,5-difluorobenzenesulfonyl Chloride | HCID 574590 | — |
| Reactant | 5-Acetyl-2-amino-4-methylthiazole | HCID 720882 | — |
| Product | HCID 11200726 | HCID 11200726 | — |
Reaction Steps
The title compound was prepared from 5-acetyl-2-amino-4-methylthiazole (42 mg) and 4-bromo-2,5-difluorobenzenesulfonyl chloride (79 mg) as described in the synthetic METHOD B to give a white solid (21.0 mg) with purty >90%: MS (pos) m/z 411.2, 413.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07125900B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-998a0c4ca70143438884655d563ed6c4 |
| Source note | uspto-grants-2006_10 |