HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Dichlorobenzenesulfonylchloride → HCID 11187666, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Dichlorobenzenesulfonylchloride | HCID 522183 | — |
| Reactant | 5-Acetyl-2-amino-4-methylthiazole | HCID 720882 | — |
| Product | HCID 11187666 | HCID 11187666 | — |
Reaction Steps
The title compound was prepared from 5-acetyl-2-amino-4-methylthiazole (42 mg) and-2,6-dichlorobenzenesulfonyl chloride (66 mg) as described in the synthetic METHOD B to give a white solid (21.4 mg) with purity >90%: MS (pos) m/z 365.3, 367.3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07125900B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-ecaaf6b164144becb8c77fb892249d59 |
| Source note | uspto-grants-2006_10 |