HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2-amino-4-methylthiazole-5-carboxylate → HCID 10158399, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2-amino-4-methylthiazole-5-carboxylate | HCID 343747 | — |
| Reactant | 2,4-Dichloro-6-methylbenzenesulfonyl chloride | HCID 2801387 | — |
| Product | HCID 10158399 | HCID 10158399 | — |
Reaction Steps
This compound was prepared from ethyl 2-amino-4-methylthiazole-5-carboxylate and 2,4-dichloro-6-methylbenzenesulfonyl chloride as described for EXAMPLE 30. Yield 254 mg, 62%: 1H NMR (DMSO) δ 7.64 (d, 1H), 7.53 (d, 1H), 4.22 (q, 2H), 2.67 (s, 3H), 2.41 (s, 3H), 1.25 (t, 3H); MS-ES (neg) In/z 407.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07125900B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-3e40ed7a5e14422990b5a4a8536fcace |
| Source note | uspto-grants-2006_10 |