HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 4777742, compound → HCID 10035419, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 4777742 | HCID 4777742 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 10035419 | HCID 10035419 | 95% |
Reaction Steps
A suspension of 1-methyl-2-carbamoyl-5-benzyloxy-1H-indole (1.94 g; 6.96 mmol) and 10% Pd/C (0.5 g) in methanol (100 ml) was hydrogenated for 2 hours. After filtration of the catalyst on celite, the filtrate was evaporated to give 1-methyl-2-carbamoyl-5-hydroxy-1H-indole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07125906B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-9b84bcdd5cde4b7da37c34d44db5ee54 |
| Source note | uspto-grants-2006_10 |