HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 4777811, compound → HCID 21915685, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 4777811 | HCID 4777811 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21915685 | HCID 21915685 | 100% |
Reaction Steps
2-Carbamoyl-5-benzyloxy-1H-indole (1 g; 3.35 mmol) in solution in methanol (60 ml) was hydrogenated on 10% Pd/C (0.28 g) for 2 hours. After filtration on celite the solvent was evaporated to give 2-carbamoyl-5-hydroxy-1H-indole which was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07125906B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-45a0c372862440a596511110a38db176 |
| Source note | uspto-grants-2006_10 |