HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-[2-[4-(2-CHLOROACETYL)PHENYL]ETHYL]ACETAMIDE → HCID 21914684, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-[2-[4-(2-CHLOROACETYL)PHENYL]ETHYL]ACETAMIDE | HCID 2468242 | — |
| Reactant | Thiourea | HCID 2723790 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21914684 | HCID 21914684 | 90.4% |
Reaction Steps
N-{2-[4-(2-Chloroacetyl)phenyl]ethyl}acetamide (1.06 g) and thiourea (505 mg) were dissolved in ethanol (20 mL). The mixture was refluxed for 1 hour and allowed to cool to room temperature. The white solid was collected with filtration and washed with ethanol to give N-{2-[4-(2-amino-1,3-thiazol-4-yl)phenyl]ethyl}acetamide hydrochloride (1.19 g, 90.4%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07125901B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-b10eb8a6261e4fcda0297c8253564d85 |
| Source note | uspto-grants-2006_10 |