HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dichlorophenol → 4-(3,4-Dichlorophenoxy)nicotinaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dichlorophenol | HCID 7258 | — |
| Reactant | 4-Chloropyridine-3-carbaldehyde | HCID 14046674 | — |
| Product | 4-(3,4-Dichlorophenoxy)nicotinaldehyde | HCID 21904690 | — |
Reaction Steps
The title compound was prepared according to Preparation 65 starting from 3,4-dichlorophenol and 4-chloronicotinaldehyde (prepared according to D. Albanese, M. Penso, M. Zenoni, Synthesis 1999, 1294–1296); δH (CDCl3, 400 MHz) 6.71 (1H, d), 7.04 (1H, dd), 7.27 (1H, m), 7.55 (1H, d), 8.02 (1H, s), 8.60 (1H, dd), 10.54 (1H, s); MS rn/z268 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07129234B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-6380928bdfb649e4a182385cd4c4c1ae |
| Source note | uspto-grants-2006_10 |