HRID1247010

反应详情

EQUATION

反应方程式

HRID 1247010 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a solution of the product from Step E (60 mg, 0.157 mmol) in methanol (10 mL) was added 10% palladium-on-carbon (20 mg) and the mixture was stirred under an atmosphere of hydrogen at room temperature for 18 h. The reaction mixture was filtered and evaporated to a colorless oil (30 mg): LC/MS m/z 247.

WORKUP

后处理

  1. filtrationThe reaction mixture was filtered
  2. customevaporated to a colorless oil (30 mg)