HCID 136335136, compound → HCID 136335137, compound

Participants

Reaction Steps

To a solution of the product from Step B (1.84 g, 7.76 mmol) in methanol (20 mL) was added palladium-on-carbon (100 mg) and this mixture was stirred under a hydrogen atmosphere at room temperature for 4 h. The reaction mixture was filtered (avoiding air) and evaporated to a colorless oil: LC/MS m/z 208. This oil was immediately carried into the next step.

Provenance & Evidence