HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69290539, compound → HCID 69288839, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69290539 | HCID 69290539 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 69288839 | HCID 69288839 | 99.1% |
Reaction Steps
To a stirred solution of (RS)-(3-benzyloxy-4-methoxy-phenyl)-methoxy-acetic acid (0.923 g) at rt in ethanol was added 10% Pd/C. The mixture was then stirred at rt under a hydrogen atmosphere for 17 h. The catalyst was filtered off and washed with dichloromethane. The filtrate was concentrated (rotavapor) to give (RS)-(3-hydroxy-4-methoxy-phenyl)-methoxy-acetic acid (0.642 g) as an orange gum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07129238B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-3b3e140a229f4937bf827859bba92e6a |
| Source note | uspto-grants-2006_10 |