HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 69290642, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 21905516 | HCID 21905516 | — |
| Product | HCID 69290642 | HCID 69290642 | — |
Reaction Steps
In analogy to example 87.2 (RS)-2-(3-aminomethyl-2,6-difluoro-phenyl)-N-(4-cyano-benzyl)-2-ethoxy-acetamide acetic acid was reacted with acetyl chloride to give (RS)-2-[3-(acetylamino-methyl)-2,6-difluoro-phenyl]-N-(4-cyano-benzyl)-2-ethoxy-acetamide. White foam. MS 402.5 ([M+H]+)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07129238B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-807e1e38d39a4e5287b473e762c116e1 |
| Source note | uspto-grants-2006_10 |