HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoic acid, 2-iodo-, methyl ester → HCID 21907643, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoic acid, 2-iodo-, methyl ester | HCID 69132 | — |
| Reactant | 2-Formyl-4-methoxybenzeneboronic acid | HCID 2734365 | — |
| Product | HCID 21907643 | HCID 21907643 | — |
Reaction Steps
Methyl 2-iodobenzoate was coupled to 2-formyl-4-methoxyphenylboronic acid using the procedure described in Example 4, Part A to provide methyl 2-(2′-formyl-4′-methoxyphenyl)benzoate. 1HNMR (300 MHz, CDCl3) δ 9.74 (s, 1H); 8.02 (d, 1H, J=7.7 Hz); 7.57 (t, 1H J=7.7 Hz); 7.50 (m, 2H); 7.28, 1, m); 7.17 (s, 2H); 3.91 (s, 3H); 3.64 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07129264B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-7e3df3f8267f4e389575a09429a5b5f0 |
| Source note | uspto-grants-2006_10 |