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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1247552Generated: October 30, 2026

HCID 69516493, compound → HCID 86595446, compound

https://huagongshe.com/reaction/1247552

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 69516493HCID 69516493—
ReactantHCID 69516804HCID 69516804—
SolventEthyl acetate hexaneHCID 21226206—
ProductHCID 86595446HCID 86595446—

Reaction Steps

From the mother liquor, after chromatography on silica gel with hexane-ethyl acetate (8:1), another 500 mg of 4-(5-fluoro-2-nitrophenyl)-2-hydroxy-4-methyl-2-trifluoromethylvaleric acid-ethyl ester accumulates as a first fraction, and 800 mg of 4-(3-fluoro-4-nitrophenyl)-2-hydroxy-4-methyl-2-trifluoromethylvaleric acid-ethyl ester as an oil accumulates as a second fraction.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07129270B2
Source datasetuspto-grants-2006_10
ORD IDord-1b826c26ad3f400d891ffe1f0b72edae
Source noteuspto-grants-2006_10