Hydrochloric Acid → HCID 21906685, compound

Participants

Reaction Steps

tert-Butyl 3-[(4-{[(1-adamantylmethyl)amino]carbonyl}-3-chloropyridin-2-yl)amino]propylcarbamate (0.41 g) Example 36(i)) in methanol (15 ml) was treated with a solution of HCl in 1,4-dioxane (4 ml) and the mixture was stirred at room temperature for 18 hrs. The solution was evaporated. Methanol was added and the solution was evaporated to give the title compound as a pale yellow solid.

Provenance & Evidence