Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 3-Aminopyridine | HCID 10009 | — |
| Reactant | HCID 23713651 | HCID 23713651 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 23713652 | HCID 23713652 | 58.9% |
Reaction Steps
A mixture of 3-aminopyridine (2.82 g) and sodium hydroxymethanesulfonate monohydrate (9.12 g) in water (40 ml) was stirred for 1.5 hours at 80° C. The solution was concentrated to yield a precipitate and stood for several hours. The resulting precipitate was filtered, washed with ethanol and dried to give sodium 3-pyridylaminomethanesulfonate (3.71 g), mp 211° to 220° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04521413 |
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| Source dataset | uspto-grants-1985_06 |
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| ORD ID | ord-281ec7f184334710b9b26d2008fc192a |
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| Source note | uspto-grants-1985_06 |
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