HRID1247946
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
A mixture of 0.01 mole of 3-chloro-3-phenyl-2-propenal and 0.01 mole of (3-amino-1H-pyrazol-4-yl)phenyl-methanone in 25 ml of acetic acid was refluxed for 6 hours. The solvent was removed in vacuo and the product isolated as described in Example 1, giving the desired product as crystals, mp 163°-165° C.
WORKUP
后处理
- temperaturewas refluxed for 6 hours
- customThe solvent was removed in vacuo
- customthe product isolated