HRID1247946

反应详情

EQUATION

反应方程式

HRID 1247946 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of 0.01 mole of 3-chloro-3-phenyl-2-propenal and 0.01 mole of (3-amino-1H-pyrazol-4-yl)phenyl-methanone in 25 ml of acetic acid was refluxed for 6 hours. The solvent was removed in vacuo and the product isolated as described in Example 1, giving the desired product as crystals, mp 163°-165° C.

WORKUP

后处理

  1. temperaturewas refluxed for 6 hours
  2. customThe solvent was removed in vacuo
  3. customthe product isolated