HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-3-phenyl-2-propenal → Phenyl(7-phenylpyrazolo[1,5-a]pyrimidin-3-yl)methanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-3-phenyl-2-propenal | HCID 38389 | — |
| Reactant | HCID 178509267 | HCID 178509267 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | Phenyl(7-phenylpyrazolo[1,5-a]pyrimidin-3-yl)methanone | HCID 13475886 | — |
Reaction Steps
A mixture of 0.01 mole of 3-chloro-3-phenyl-2-propenal and 0.01 mole of (3-amino-1H-pyrazol-4-yl)phenyl-methanone in 25 ml of acetic acid was refluxed for 6 hours. The solvent was removed in vacuo and the product isolated as described in Example 1, giving the desired product as crystals, mp 163°-165° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04521422 |
| Source dataset | uspto-grants-1985_06 |
| ORD ID | ord-ce205ec633b54248a0728969eba33ce2 |
| Source note | uspto-grants-1985_06 |