HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Acetylpyridine → HCID 54355643, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Acetylpyridine | HCID 9589 | — |
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 54355643 | HCID 54355643 | — |
Reaction Steps
A mixture of 0.10 mole of 3-acetylpyridine and 0.10 mole of N,N-dimethylformamide dimethylacetal in 100 ml of benzene was refluxed for 12 hours. The solvent was removed, giving 3-dibutylamino-1-(3-pyridinyl)-2-propen-1-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04521422 |
| Source dataset | uspto-grants-1985_06 |
| ORD ID | ord-67d2d75d53514a2a9a5e829fec826ab3 |
| Source note | uspto-grants-1985_06 |