HRID1247956

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID9589

3-Acetylpyridine

C7H7NO

HCID12747026

N-(Dimethoxymethyl)-N-ethylethanamine

C7H17NO2

PRODUCTS

生成物

HCID54453514

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID31275

1,4-Dioxane

C4H8O2

PROCEDURE

实验过程

A mixture of 0.10 mole of 3-acetylpyridine and 0.10 mole of N,N-diethylformamide dimethylacetal in 100 ml of dioxane was refluxed for 10 hours. The solvent was removed, giving 3-diethylamino-1-(3-pyridinyl)-2-propen-1-one.

WORKUP

后处理

temperaturewas refluxed for 10 hours
customThe solvent was removed