HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Acetylpyridine → 3-Diethylamino-1-(3-pyridinyl)-2-propen-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Acetylpyridine | HCID 9589 | — |
| Reactant | N-(Dimethoxymethyl)-N-ethylethanamine | HCID 12747026 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 3-Diethylamino-1-(3-pyridinyl)-2-propen-1-one | HCID 54453514 | — |
Reaction Steps
A mixture of 0.10 mole of 3-acetylpyridine and 0.10 mole of N,N-diethylformamide dimethylacetal in 100 ml of dioxane was refluxed for 10 hours. The solvent was removed, giving 3-diethylamino-1-(3-pyridinyl)-2-propen-1-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04521422 |
| Source dataset | uspto-grants-1985_06 |
| ORD ID | ord-f251af5646414a149ab646cab16b7be3 |
| Source note | uspto-grants-1985_06 |