HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1247957Generated: November 3, 2026
3-Acetylpyridine → 1-(3-Pyridyl)-3-(dimethylamino)-2-propen-1-one
https://huagongshe.com/reaction/1247957
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 3-Acetylpyridine | HCID 9589 | — |
| Reactant | 1,1-Dipropoxytrimethylamine | HCID 80105 | — |
| Product | 1-(3-Pyridyl)-3-(dimethylamino)-2-propen-1-one | HCID 567033 | — |
Reaction Steps
A mixture of 25 g of 3-acetylpyridine and 35 ml of N,N-dimethylformamide dipropylacetal was heated at 100° C. for 6 hours. The mixture was concentrated in vacuo and the residue crystallized, giving 3-dimethylamino-1-(3-pyridinyl)-2-propen-1-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04521422 |
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| Source dataset | uspto-grants-1985_06 |
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| ORD ID | ord-87f549b9bb1f4a51b634f750a76c3a45 |
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| Source note | uspto-grants-1985_06 |
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