HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Acetylpyridine → 1-(3-Pyridyl)-3-(dimethylamino)-2-propen-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Acetylpyridine | HCID 9589 | — |
| Reactant | tert-Butoxy bis(dimethylamino)methane | HCID 79885 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 1-(3-Pyridyl)-3-(dimethylamino)-2-propen-1-one | HCID 567033 | — |
Reaction Steps
To a mixture of 0.10 mole of 3-acetylpyridine in 100 ml of tetrahydrofuran was added 0.10 mole of tert.-butoxy-bis-(dimethylamino)methane. The mixture was stirred for 24 hours and the solvent removed, giving 3-dimethylamino-1-(3-pyridinyl)-2-propen-1-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04521422 |
| Source dataset | uspto-grants-1985_06 |
| ORD ID | ord-66a7bcd24824440ba61d4ed7dbafb609 |
| Source note | uspto-grants-1985_06 |