HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Acetylpyridine → 2-Propen-1-one, 3-(dimethylamino)-1-(4-pyridinyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Acetylpyridine | HCID 14282 | — |
| Reactant | 1,1-Bis(benzyloxy)trimethylamine | HCID 74837 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 2-Propen-1-one, 3-(dimethylamino)-1-(4-pyridinyl)- | HCID 714531 | — |
Reaction Steps
A mixture of 0.10 mole of 4-acetylpyridine and 0.12 mole of N,N-dimethylformamide dibenzylacetal in benzene was refluxed for 8 hours, giving 3-dimethylamino-1-(4-pyridinyl)-2-propen-1-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04521422 |
| Source dataset | uspto-grants-1985_06 |
| ORD ID | ord-f1d28c0bd68a4738905a0332c1d8d1f9 |
| Source note | uspto-grants-1985_06 |