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HRID1247960

反应详情

EQUATION

反应方程式

HRID 1247960 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)c1ccncc1
HCID14282

4-Acetylpyridine

C7H7NO

结构：CN(C)C(OCc1ccccc1)OCc1ccccc1
HCID74837

1,1-Bis(benzyloxy)trimethylamine

C17H21NO2

PRODUCTS

生成物

1
结构：CN(C)C=CC(=O)c1ccncc1
HCID714531

2-Propen-1-one, 3-(dimethylamino)-1-(4-pyridinyl)-

C10H12N2O

AUXILIARIES

试剂、催化剂与溶剂

1
结构：c1ccccc1
溶剂HCID241

Benzene

C6H6

PROCEDURE

实验过程

A mixture of 0.10 mole of 4-acetylpyridine and 0.12 mole of N,N-dimethylformamide dibenzylacetal in benzene was refluxed for 8 hours, giving 3-dimethylamino-1-(4-pyridinyl)-2-propen-1-one.

WORKUP

后处理

  1. temperaturewas refluxed for 8 hours