HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide dimethyl acetal → N-[3-(3-Dimethylaminoacryloyl)phenyl]acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | 3'-Acetamidoacetophenone | HCID 346202 | — |
| Product | N-[3-(3-Dimethylaminoacryloyl)phenyl]acetamide | HCID 53412415 | — |
Reaction Steps
A 30.0 g portion of 3-acetamidoacetophenone was heated with 50 ml of dimethylformamide dimethylacetal on a steam bath under inert atmosphere for 8 hours. After cooling, the precipitated material was collected by filtration to yield the desired material as orange crystals (37.20 g, mp 184°-185° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04521422 |
| Source dataset | uspto-grants-1985_06 |
| ORD ID | ord-5fcaa470b9464e26b9a06defddd59089 |
| Source note | uspto-grants-1985_06 |