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HRID1247969

反应详情

EQUATION

反应方程式

HRID 1247969 的结构方程式

REACTANTS

反应物

2
结构：COC(OC)N(C)C
HCID78373

Methanamine, 1,1-dimethoxy-N,N-dimethyl-

C5H13NO2

结构：CC(=O)Nc1cccc(C(C)=O)c1
HCID346202

3'-Acetamidoacetophenone

C10H11NO2

PRODUCTS

生成物

1
结构：CC(=O)Nc1cccc(C(=O)C=CN(C)C)c1
HCID53412415

未命名化合物

PROCEDURE

实验过程

A 30.0 g portion of 3-acetamidoacetophenone was heated with 50 ml of dimethylformamide dimethylacetal on a steam bath under inert atmosphere for 8 hours. After cooling, the precipitated material was collected by filtration to yield the desired material as orange crystals (37.20 g, mp 184°-185° C.).

WORKUP

后处理

  1. temperatureAfter cooling
  2. filtrationthe precipitated material was collected by filtration