HRID1248196

反应详情

EQUATION

反应方程式

HRID 1248196 的结构方程式

PROCEDURE

实验过程

3-(Cyclohexylmethyl)heptanenitrile (1.43 g) in 10 ml of 50% aqueous sulfuric acid was heated under reflux overnight. The cooled mixture was then poured into water (100 ml) and extracted twice with ether. The ethereal extracts were washed with water, dried (MgSO4) and evaporated to give 3-(cyclohexylmethyl)heptanoic acid.

WORKUP

后处理

  1. temperatureunder reflux overnight
  2. extractionextracted twice with ether
  3. washThe ethereal extracts were washed with water
  4. dry with materialdried (MgSO4)
  5. customevaporated