HRID1248196
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
3-(Cyclohexylmethyl)heptanenitrile (1.43 g) in 10 ml of 50% aqueous sulfuric acid was heated under reflux overnight. The cooled mixture was then poured into water (100 ml) and extracted twice with ether. The ethereal extracts were washed with water, dried (MgSO4) and evaporated to give 3-(cyclohexylmethyl)heptanoic acid.
WORKUP
后处理
- temperatureunder reflux overnight
- extractionextracted twice with ether
- washThe ethereal extracts were washed with water
- dry with materialdried (MgSO4)
- customevaporated