HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 3-(Cyclohexylmethyl)heptanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 3-(Cyclohexylmethyl)heptanenitrile | HCID 20279061 | — |
| Product | 3-(Cyclohexylmethyl)heptanoic acid | HCID 20279056 | — |
Reaction Steps
3-(Cyclohexylmethyl)heptanenitrile (1.43 g) in 10 ml of 50% aqueous sulfuric acid was heated under reflux overnight. The cooled mixture was then poured into water (100 ml) and extracted twice with ether. The ethereal extracts were washed with water, dried (MgSO4) and evaporated to give 3-(cyclohexylmethyl)heptanoic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04522948 |
| Source dataset | uspto-grants-1985_06 |
| ORD ID | ord-186a570d2f634d30a9148c3d2213196f |
| Source note | uspto-grants-1985_06 |