Potassium Carbonate → HCID 13476555, compound

HRID 1248200Notes

Reaction equation

HRID 1248200 reaction equation
S(O)(O)(=O)=O.[CH:6]1([CH2:12][CH:13]([CH2:20][CH2:21][CH2:22][CH3:23])[CH2:14][N:15]2[CH:19]=[CH:18][N:17]=[CH:16]2)[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7]1.C(=O)([O-])[O-].[K+].[K+]>CCOCC>[CH:6]1([CH2:12][CH:13]([CH2:20][CH2:21][CH2:22][CH3:23])[CH2:14][N:15]2[CH:19]=[CH:18][N:17]=[CH:16]2)[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11]1

Participants

4

Reactant 2

HCID 11430Potassium CarbonateHCID 13476556HCID 13476556, compound

Product 1

HCID 13476555HCID 13476555, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

A mixture of 1.0 g of 1-[2-(cyclohexylmethyl)-n-hexyl]imidazole hydrogen sulfate, ether (50 ml) and excess aqueous potassium carbonate was stirred until no solid remained. The ether layer was separated, washed with water, dried (MgSO4) and evaporated to give 1-[2-(cyclohexylmethyl)-n-hexyl]imidazole as an oil.

Workup

  1. customThe ether layer was separated
  2. washwashed with water
  3. dry with materialdried (MgSO4)
  4. customevaporated

Sources & evidence

ORD record
ord-897a2739cbe14f42bf803d0b6b5e4223
Source dataset
uspto-grants-1985_06
Patent number
US04522948

Reaction notes

Loading…