Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 1-Hexylpiperazine | HCID 2736513 | — |
| Reactant | 1-Chlorohexan-3-one | HCID 13458588 | — |
| Product | HCID 70477224 | HCID 70477224 | — |
Reaction Steps
A mixture of 1.8 g (0.01 mole) of n-hexyl piperazine and 1.9 g (0.014 mole) of 1-chloro-3-hexanone was heated to 120° C. for 5 minutes. The reaction product was slurried with ether, filtered and crystallized from acetonitrile to yield 4.2 g of product having a melting point of 162°-164° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04523014 |
|---|
| Source dataset | uspto-grants-1985_06 |
|---|
| ORD ID | ord-a8738ba4fd494fac813d1a55f6e31862 |
|---|
| Source note | uspto-grants-1985_06 |
|---|
